Cobalt-free perovskite Pr0.5Sr0.5Fe1 xCuxO3 d(PSFC) as a cathodematerial for intermediate temperature solid oxide fuel cells

SFC (Pr0.5Sr0.5Fe1 xCuxO3 d) is a new perovskite-type oxide that has gained considerable attention ascathode material for intermediate temperature solid oxide fuel cells (IT-SOFCs), due to its high mixedionic-electronic conductivity below 800 C. In this work, PSFC (Pr0.5Sr0.5Fe1 xCuxO3 d,x¼0.2 and 0...

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Detalhes bibliográficos
Autores: Nascimento, Rubens Maribondo do, Moura, Caroline Gomes, Fagg, Duncan Paul, Grilo, João Paulo de Freitas, Macedo, Daniel Araújo de, Cesário, Moises Rômolos
Formato: artículo
Estado:Versión publicada
Fecha de publicación:2016
País:Brasil
Recursos:Universidade Federal do Rio Grande do Norte (UFRN)
Repositorio:Repositório Institucional da UFRN
Idioma:inglés
OAI Identifier:oai:repositorio.ufrn.br:123456789/45570
Acesso em linha:https://repositorio.ufrn.br/handle/123456789/45570
Access Level:acceso abierto
Palavra-chave:Oxides
Chemical synthesis
Impedance spectroscopy
X-ray diffraction
Thermal expansion
Descrição
Resumo:SFC (Pr0.5Sr0.5Fe1 xCuxO3 d) is a new perovskite-type oxide that has gained considerable attention ascathode material for intermediate temperature solid oxide fuel cells (IT-SOFCs), due to its high mixedionic-electronic conductivity below 800 C. In this work, PSFC (Pr0.5Sr0.5Fe1 xCuxO3 d,x¼0.2 and 0.4)powders were synthesized by the citrate method and structurally characterized by X-ray diffractometry.Screen-printed cathodes were sintered at 1050 C and electrochemically characterized by impedancespectroscopy at 600e800 C in pure oxygen. The area specific resistances (ASR) of thePr0.5Sr0.5Fe0.8Cu0.2O3 dmaterial are shown to be competitive with typical values reported for cobalt-based cathodes in the measured temperature range, while, importantly, offering a significantly loweractivation energy, 0.62 eV. The thermal expansion coefficients of these Co-free cathodes are in the rangeof 13e15 10 6 C 1, in a temperature range 200e650 C, demonstrating a good thermal compatibilitywith gadolinia doped ceria (CGO) electrolytes