Thiol Adsorption on the Au(100)-hex and Au(100)-(1 × 1) Surfaces

Alkanethiol adsorption on the Au(100) surfaces is studied by using scanning tunneling microscopy, X-ray photoelectron spectroscopy, and electrochemical techniques. Adsorption of hexanethiol (HT) on the Au(100)-hex surface results in the formation of elongated Au islands following the typical stripes...

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Detalles Bibliográficos
Autores: Grumelli, Doris Elda, Cristina, Lucila Josefina, Lobo Maza, Flavia Emilia, Carro, Pilar, Ferron, Julio, Kern, Klaus, Salvarezza, Roberto Carlos
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2015
País:Argentina
Institución:Consejo Nacional de Investigaciones Científicas y Técnicas
Repositorio:CONICET Digital (CONICET)
Idioma:inglés
OAI Identifier:oai:ri.conicet.gov.ar:11336/30257
Acceso en línea:http://hdl.handle.net/11336/30257
Access Level:acceso abierto
Palabra clave:Hexanethiol
Au(100)
Adsorption
Surfaces
https://purl.org/becyt/ford/1.4
https://purl.org/becyt/ford/1
Descripción
Sumario:Alkanethiol adsorption on the Au(100) surfaces is studied by using scanning tunneling microscopy, X-ray photoelectron spectroscopy, and electrochemical techniques. Adsorption of hexanethiol (HT) on the Au(100)-hex surface results in the formation of elongated Au islands following the typical stripes of the reconstruction. Ordered molecular arrays forming hexagonally distorted square patterns cover the stripes with surface coverage ≈0.33. On the other hand, HT adsorption on the Au(100)-(1 × 1) surface shows the absence of the elongated island and the formation of square molecular patterns with a surface coverage ≈0.44. The core level shift of thiolates adsorbed on the Au(100)-(1 × 1) and Au(111) is only 0.15 eV, suggesting that chemistry rather than surface sites determines the binding energy of the S 2p core level. These results are also important to complete our knowledge of the chemistry and surface structure for small thiolated AuNPs where the Au(100) together with the Au(111) are the dominant faces.