Supercritical fluid extraction of alkaloids from Ilex paraguariensis St. Hil.

In this work a study about extracts obtained from Ilex paraguariensis St. Hil. leaves with supercritical CO2 was carried out. Experiments were performed in a pilot-scale extractor with capacity of 1 L at pressure of 120, 150, 170 and 200 bar for four temperature conditions, 313.15, 323.15, 333.15 an...

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Detalles Bibliográficos
Autores: Cassel, Eduardo, Vargas, Rubem Mário Figueiró, Brun, Gerti Weber, Almeida, Diego Erthal, Cogoi, Laura Carolina, Ferraro, Graciela Ester, Filip, Rosana
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2010
País:Argentina
Institución:Consejo Nacional de Investigaciones Científicas y Técnicas
Repositorio:CONICET Digital (CONICET)
Idioma:inglés
OAI Identifier:oai:ri.conicet.gov.ar:11336/67572
Acceso en línea:http://hdl.handle.net/11336/67572
Access Level:acceso abierto
Palabra clave:Alkaloids
Caffeine
Ilex Paraguariensis St. Hil.
Mathematical Model
Supercritical Extraction
https://purl.org/becyt/ford/3.3
https://purl.org/becyt/ford/3
Descripción
Sumario:In this work a study about extracts obtained from Ilex paraguariensis St. Hil. leaves with supercritical CO2 was carried out. Experiments were performed in a pilot-scale extractor with capacity of 1 L at pressure of 120, 150, 170 and 200 bar for four temperature conditions, 313.15, 323.15, 333.15 and 343.15 K. The experimental data were fitted using a mathematical model characterized by the existence of two distinct periods of extraction. Numerical results for the adjusted parameters correlated very well the supercritical extraction experimental data. The confidence of results obtained from mathematical model and experiments was assured through the chi-square test.