On the Nature of Defects in Liquid-Phase Exfoliated Graphene

Liquid-phase exfoliation is one of the most promising routes for large-scale production of multilayer graphene dispersions. These dispersions, which may be used in coatings, composites, or paints, are believed to contain disorder-free graphene multilayers. Here, we address the nature of defects in s...

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Detalles Bibliográficos
Autores: Bracamonte, Maria Victoria, Lacconi, Gabriela Ines, Urreta, Silvia Elena, Foa Torres, Luis Eduardo Francisco
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2014
País:Argentina
Institución:Consejo Nacional de Investigaciones Científicas y Técnicas
Repositorio:CONICET Digital (CONICET)
Idioma:inglés
OAI Identifier:oai:ri.conicet.gov.ar:11336/31375
Acceso en línea:http://hdl.handle.net/11336/31375
Access Level:acceso abierto
Palabra clave:Graphene
Liquid-Phase Exfoliation
Edges Defects
https://purl.org/becyt/ford/1.3
https://purl.org/becyt/ford/1
Descripción
Sumario:Liquid-phase exfoliation is one of the most promising routes for large-scale production of multilayer graphene dispersions. These dispersions, which may be used in coatings, composites, or paints, are believed to contain disorder-free graphene multilayers. Here, we address the nature of defects in such samples obtained by liquid-phase exfoliation of graphite powder in N-methyl-2-pyrrolidone. Our Raman spectroscopy data challenge the assumption that these multilayers are free of bulk defects, revealing that defect localization strongly depends on the sonication time. For short ultrasound times, defects are located mainly at the layer edges but they turn out to build up in the bulk for ultrasonic times above 2 h. This knowledge may help to devise better strategies to achieve high-quality graphene dispersions.