Thiosaccharine disulfide: Synthesis, crystal structure, spectroscopic characterization and theoretical study

The title compound, (thiosaccharine disulfide), bis[1,10dioxide-2,3-dihidro-1,2-benzoisothiazol]disulfide,(tsac)2 has been synthesized and fully characterized by UV?Visible, IR, Raman, 1H and 13C NMR spectroscopy elemental analysis and structural X-ray crystallography. A DFT theoretical study has be...

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Detalles Bibliográficos
Autores: Ferullo, Ricardo, Granados, Alejandro Manuel, Lanterna, Anabel Estela, Guida, Jorge Alberto, Piro, Oscar Enrique, Castellano, Eduardo E., Dennehy, Mariana
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2013
País:Argentina
Institución:Consejo Nacional de Investigaciones Científicas y Técnicas
Repositorio:CONICET Digital (CONICET)
Idioma:inglés
OAI Identifier:oai:ri.conicet.gov.ar:11336/7628
Acceso en línea:http://hdl.handle.net/11336/7628
Access Level:acceso abierto
Palabra clave:Thiosaccharine
Disulfide
Crystal Structure
Infrared
Raman
Uv-Visible Spectroscopy
https://purl.org/becyt/ford/1.4
https://purl.org/becyt/ford/1
Descripción
Sumario:The title compound, (thiosaccharine disulfide), bis[1,10dioxide-2,3-dihidro-1,2-benzoisothiazol]disulfide,(tsac)2 has been synthesized and fully characterized by UV?Visible, IR, Raman, 1H and 13C NMR spectroscopy elemental analysis and structural X-ray crystallography. A DFT theoretical study has been performed and good agreement between experimental and theoretical values of structural parameters and vibration frequencies have been achieved.

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