Oxidative dehydrogenation of propane and n-butane over alumina supported vanadium catalysts

Structural properties of vanadium dispersed species on γ-A1203 are investigated with the scope to detect changes related with V loading in the oxidative dehydrogenation (ODH) of propane and nbutane. XPS, FTIR, and FTIR of absorbed pyridine were used to study the nature of vanadium supported species....

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Detalhes bibliográficos
Autores: Murgia, Viviana, Sham, Edgardo Ling, Gottifredi, Juan Carlos Agustin, Farfan Torres, Elsa Monica
Formato: artículo
Estado:Versión publicada
Fecha de publicación:2004
País:Argentina
Recursos:Consejo Nacional de Investigaciones Científicas y Técnicas
Repositorio:CONICET Digital (CONICET)
Idioma:inglés
OAI Identifier:oai:ri.conicet.gov.ar:11336/72764
Acesso em linha:http://hdl.handle.net/11336/72764
Access Level:acceso abierto
Palavra-chave:Oxidative Dehydrogenation
Vanadium Catalysts
Propane
N-Butane
https://purl.org/becyt/ford/2.11
https://purl.org/becyt/ford/2
Descrição
Resumo:Structural properties of vanadium dispersed species on γ-A1203 are investigated with the scope to detect changes related with V loading in the oxidative dehydrogenation (ODH) of propane and nbutane. XPS, FTIR, and FTIR of absorbed pyridine were used to study the nature of vanadium supported species. Tetrahedral V5+ and probably V4+ species were detected. For vanadium loadings higher than 4.3 % wt octahedral species were also observed. In the n-butane ODH reaction, the selectivity to ODH products decreases when vanadium content increases. However, for propane ODH, the selectivity seems to be independent of vanadium loadings. Low oxygen/alkane feeding ratios favor selectivity to olefins. It is also shown that low V loading catalysts reach selectivities as good as best reported V-Mg-O catalyst.