Optimization of β-cyclodextrin-based extraction of antioxidant and anti-browning activities from thyme leaves by response surface methodology

Thyme (Thymus vulgaris) has been demonstrated to extend the shelf-life of food products, being also a potential source of bioactive compounds. The aim of this research was to optimize the ultrasound assisted extraction employing β-cyclodextrin aqueous solutions as no-contaminant technology and Respo...

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Detalles Bibliográficos
Autores: Favre, Leonardo Cristian, dos Santos, Cristina, Lopez Fernandez, Maria Paula, Mazzobre, Maria Florencia, Buera, Maria del Pilar
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2018
País:Argentina
Institución:Consejo Nacional de Investigaciones Científicas y Técnicas
Repositorio:CONICET Digital (CONICET)
Idioma:inglés
OAI Identifier:oai:ri.conicet.gov.ar:11336/96209
Acceso en línea:http://hdl.handle.net/11336/96209
Access Level:acceso abierto
Palabra clave:2,2-DIPHENYL-1-PICRYLHYDRAZYL RADICAL (DPPH[RAD]) (PUBCHEM CDI: 2735032)
2,4,6-TRIPYRIDYL-S-TRIAZINE (TPTZ) (PUBCHEM CID: 77258)
ANTI-GLYCATION
ANTIOXIDANT ACTIVITY
BOVINE SERUM ALBUMIN (BSA) (PUBCHEM CID: 16132389)
FERRIC CHLORIDE HEXAHYDRATE (PUBCHEM CID: 6093258)
GALLIC ACID (PUBCHEM CID: 370)
GLUCOSE (PUBCHEM CID: 5793)
MAILLARD
PHOSPHATE BUFFERED SALINE (PBS) (PUBCHEM CID: 24978514)
SODIUM CARBONATE TRIHYDRATE (PUBCHEM CID: 10340)
THYME
ULTRASONIC
Β-CYCLODEXTRIN
Β-CYCLODEXTRIN (Β-CD) (PUBCHEM CID: 444041)
https://purl.org/becyt/ford/1.4
https://purl.org/becyt/ford/1
Descripción
Sumario:Thyme (Thymus vulgaris) has been demonstrated to extend the shelf-life of food products, being also a potential source of bioactive compounds. The aim of this research was to optimize the ultrasound assisted extraction employing β-cyclodextrin aqueous solutions as no-contaminant technology and Response Surface Methodology to obtain thyme extracts with the maximum antioxidant capacity. The optimal extraction conditions were: a solution of β-ciclodextrin 15 mM, an ultrasonic treatment time of 5.9 min at a temperature of 36.6 °C. They resulted in an extract with a polyphenolic content of 189.3 mg GAE/mL, an antioxidant activity (DPPH[rad]) of 14.8 mg GAE/mL, and ferric reducing/antioxidant power (FRAP) of 3.3 mg GAE/mL. Interestingly, the extract demonstrated to inhibit the production of Maillard browning products and can be considered a potential antiglycant agent. The obtained data is important for developing eco-friendly technologies in order to obtain natural antioxidant extracts with a potential inhibitory capacity of Maillard glycation reaction.