Corn syrup clarification by microfiltration with ceramic membranes

The performance in clarifying corn syrup of three different microfiltration ceramic membranes made in our laboratory was investigated. From preliminary MF tests at laboratory scale, it was found that the composite ceramic membrane with average hydraulic pore size radius of rh ≈ 0.5 m (CM05) performe...

Descripción completa

Detalles Bibliográficos
Autores: Almandoz, Maria Cristina, Pagliero, Cecilia Liliana, Ochoa, Nelio Ariel, Marchese, Jose
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2010
País:Argentina
Institución:Consejo Nacional de Investigaciones Científicas y Técnicas
Repositorio:CONICET Digital (CONICET)
Idioma:inglés
OAI Identifier:oai:ri.conicet.gov.ar:11336/104428
Acceso en línea:http://hdl.handle.net/11336/104428
Access Level:acceso abierto
Palabra clave:Microfiltration
Corn syrup
Clarification
Ceramic membrane
Membrane fouling
https://purl.org/becyt/ford/1.4
https://purl.org/becyt/ford/1
Descripción
Sumario:The performance in clarifying corn syrup of three different microfiltration ceramic membranes made in our laboratory was investigated. From preliminary MF tests at laboratory scale, it was found that the composite ceramic membrane with average hydraulic pore size radius of rh ≈ 0.5 m (CM05) performed better than the other two membranes (rh ≈ 0.14 m and rh ≈ 0.75 m). Further studies of corn syrup clarification with the CM05 membrane at bench scale, with and without air backpulsing, were performed. The effects of transmembrane pressure (p = 10.3–103.4 kPa) and the feed flow velocities (v = 1.32–3.18 m/s) on permeate flux at T = 60 ◦C were analyzed. Permeate fluxes without back-flushing decreased considerably during the first hour of operation; around 60–70% of the initial permeate flux. Membrane fouling responsible for the permeate flux decline during the operation time was evaluated by applying different blocking models and cake filtration model. Results indicate that a good fitting correlation between the experimental data and pore blocking models was achieved. When back-flushing procedure was applied high efficiency of average permeate flux (J ≈ 95–105 L/m2 h) was obtained. From these experiments, sequential back-flushing is recommended to achieve the highest flux values and allow the filtration cycle to continue over longer periods of time. The turbidity, insoluble residue, and total protein rejection performances of CM05 membrane were significantly higher than those obtained using the traditional rotary vacuum filtration (RVF) process.