Determination of the blocking temperature of magnetic nanoparticles: The good, the bad, and the ugly
A numerically solved two-level Stoner-Wohlfarth model with thermal agitation is used to simulate Zero Field Cooling (ZFC)-Field Cooling (FC) curves of monosize and polysize samples and to determine the best method for obtaining a representative blocking temperature TB value of polysize samples. The...
| Autores: | , , , , |
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| Tipo de documento: | artigo |
| Estado: | Versão publicada |
| Data de publicação: | 2015 |
| País: | Argentina |
| Recursos: | Consejo Nacional de Investigaciones Científicas y Técnicas |
| Repositório: | CONICET Digital (CONICET) |
| Idioma: | inglês |
| OAI Identifier: | oai:ri.conicet.gov.ar:11336/142870 |
| Acesso em linha: | http://hdl.handle.net/11336/142870 |
| Access Level: | Acceso aberto |
| Palavra-chave: | Blocking temperature Magnetic anisotropy Nanoparticles ZFC-FC https://purl.org/becyt/ford/2.10 https://purl.org/becyt/ford/2 |
| Resumo: | A numerically solved two-level Stoner-Wohlfarth model with thermal agitation is used to simulate Zero Field Cooling (ZFC)-Field Cooling (FC) curves of monosize and polysize samples and to determine the best method for obtaining a representative blocking temperature TB value of polysize samples. The results confirm a technique based on the T derivative of the difference between ZFC and FC curves proposed by Micha et al. (the good) and demonstrate its relation with two alternative methods: the ZFC maximum (the bad) and the inflection point (the ugly). The derivative method is then applied to experimental data, obtaining the TB distribution of a polysize Fe3O4 nanoparticle sample suspended in hexane with an excellent agreement with TEM characterization. |
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