Synthesis and Characterization of Iron Oxyhydroxide Nanowires

A very simple method of synthesis of goethite,alfa-FeOOH, nanowire is reported. To fabricate the nanowires, an anodiezed alumina nanoporous template (AAO) is used. AAO has pores with an average diameter of 60 nm. The synthesis is based on a self-combustion reaction of the chemical precursor (Fe(NO3)...

Descripción completa

Detalles Bibliográficos
Autores: Londoño Calderon, Cesar Leandro, Bilovol, Vitaliy, Cosio Castañeda, Carlos, Pampillo, Laura Gabriela, Micheli, Sabina R., Pirota, Kleber Roberto, Socolovsky, Leandro Martin, Martinez Garcia, Ricardo
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2013
País:Argentina
Institución:Consejo Nacional de Investigaciones Científicas y Técnicas
Repositorio:CONICET Digital (CONICET)
Idioma:inglés
OAI Identifier:oai:ri.conicet.gov.ar:11336/6564
Acceso en línea:http://hdl.handle.net/11336/6564
Access Level:acceso abierto
Palabra clave:Iron Oxide
Iron Oxyhydroxide
Nanowires
Structural Properties
Magnetic Properties
https://purl.org/becyt/ford/2.10
https://purl.org/becyt/ford/2
Descripción
Sumario:A very simple method of synthesis of goethite,alfa-FeOOH, nanowire is reported. To fabricate the nanowires, an anodiezed alumina nanoporous template (AAO) is used. AAO has pores with an average diameter of 60 nm. The synthesis is based on a self-combustion reaction of the chemical precursor (Fe(NO3)3 satured solution) which occurs inside the nanopores. The geometry of AAO determines the morphology of the nanowires and the confinement conditions in which the heat treatment determines the composition of the nanostruc- ture. The nanowires are characterized using scanning electronmicroscopy, high resolution transmission electronmicroscopy andmagne- tometry [magnetization versus applied field (M versus H)]. TEM analysis indicates that nanowires are composed of several alfa-FeOOH single crystals. The nanowires have a clear magnetic oriented structure.

Similares en LA Referencia