Inhibition of mild steel corrosion in HCI solution using chitosan

The efficiency of chitosan (a naturally occurring polymer) as a corrosion inhibitor for mild steel in 0.1 M HCl, was investigated by gravimetric, electrochemical and spectroscopic measurements (SEM observations and UV-visible analysis). The polymer was found to inhibit corrosion even at a very low c...

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Detalles Bibliográficos
Autores: Umoren, Saviour E., Banera, Mauro, Alonso Garcia, Teodoro, Gervasi, Claudio, Mirifico, Maria Virginia
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2013
País:Argentina
Institución:Consejo Nacional de Investigaciones Científicas y Técnicas
Repositorio:CONICET Digital (CONICET)
Idioma:inglés
OAI Identifier:oai:ri.conicet.gov.ar:11336/5139
Acceso en línea:http://hdl.handle.net/11336/5139
Access Level:acceso abierto
Palabra clave:Chitosan
Mild Steel
Acid Corrosion
Corrosion Inhibition
Natural Polymer
https://purl.org/becyt/ford/1.4
https://purl.org/becyt/ford/1
Descripción
Sumario:The efficiency of chitosan (a naturally occurring polymer) as a corrosion inhibitor for mild steel in 0.1 M HCl, was investigated by gravimetric, electrochemical and spectroscopic measurements (SEM observations and UV-visible analysis). The polymer was found to inhibit corrosion even at a very low concentration. Inhibition efficiency increases with a rise in temperature up to 96 % at 60°C and then drops to 93% at 70°C, while it slightly increases with an increase in chitosan concentration. Polarization curves indicate that chitosan functions as a mixed inhibitor, affecting both cathodic and anodic corrosion reactions. Impedance results indicate that chitosan was adsorbed on the metal/solution interface. Adsorption of chitosan at the mild steel surface is found to be in agreement with Langmuir adsorption isotherm model. Chemical adsorption is the proposed mechanism for corrosion inhibition considering the trend of protection efficiency with temperature. Calculated kinetic and thermodynamic parameters corroborate the proposed mechanism.