Conformational and electronic (AIM/NBO) study of unsubstituted A-type dimeric proanthocyanidin

The conformational space of the unsubstituted Atype dimeric proanthocyanidin was scanned using molecular dynamics at a semiempirical level, and complemented with functional density calculations. The lowest energy conformers were obtained. Electronic distributions were analysed at a higher calculatio...

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Detalles Bibliográficos
Autores: Lobayan, Rosana Maria, Jubert, Alicia Haydee, Vitale, Martín G., Pomilio, Alicia Beatriz
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2008
País:Argentina
Institución:Consejo Nacional de Investigaciones Científicas y Técnicas
Repositorio:CONICET Digital (CONICET)
Idioma:inglés
OAI Identifier:oai:ri.conicet.gov.ar:11336/102465
Acceso en línea:http://hdl.handle.net/11336/102465
Access Level:acceso abierto
Palabra clave:PROANTHOCYANIDINS
CONFORMATIONAL STUDY
ELECTRONIC STUDY
AIM/NBO
https://purl.org/becyt/ford/1.4
https://purl.org/becyt/ford/1
Descripción
Sumario:The conformational space of the unsubstituted Atype dimeric proanthocyanidin was scanned using molecular dynamics at a semiempirical level, and complemented with functional density calculations. The lowest energy conformers were obtained. Electronic distributions were analysed at a higher calculation level, thus improving the basis set. A topological study based on Bader’s theory (AIM: atoms in molecules) and natural bond orbital (NBO) framework was performed. Furthermore, molecular electrostatic potential maps (MEPs) were obtained and analysed. NMR chemical shifts were calculated at ab initio level and further compared with previous experimental values; coupling constants were also calculated. The stereochemistry of the molecule is thoroughly discussed, revealing the key role that hyperconjugative interactions play in defining experimental trends. These results show the versatility of geminal spin–spin coupling 2 J(C-1′,O) as a probe for stereochemical studies of proanthocyanidins.