6-Mercaptopurine Self-Assembled Monolayers on Gold (001)-Hex: Revealing the Fate of Gold Adatoms

Thiol molecules adsorbed on gold became a model system for molecular self-assembly on metal substrates long ago. In most cases the strong molecule-gold interaction is able to restructure the substrate, resulting in vacancy islands and steps. Today it is widely accepted that gold adatoms produced by...

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Detalhes bibliográficos
Autores: Carro, Pilar, Müller, Kathrin, Lobo Maza, Flavia Emilia, Vericat, Carolina, Starke, Ulrich, Kern, Klaus, Salvarezza, Roberto Carlos, Grumelli, Doris Elda
Formato: artículo
Estado:Versión publicada
Fecha de publicación:2017
País:Argentina
Recursos:Consejo Nacional de Investigaciones Científicas y Técnicas
Repositorio:CONICET Digital (CONICET)
Idioma:inglés
OAI Identifier:oai:ri.conicet.gov.ar:11336/63302
Acesso em linha:http://hdl.handle.net/11336/63302
Access Level:acceso abierto
Palavra-chave:self assembled monolayers
6 mercaptopurine
Au 100 5x20
STM_LEED
https://purl.org/becyt/ford/1.4
https://purl.org/becyt/ford/1
Descrição
Resumo:Thiol molecules adsorbed on gold became a model system for molecular self-assembly on metal substrates long ago. In most cases the strong molecule-gold interaction is able to restructure the substrate, resulting in vacancy islands and steps. Today it is widely accepted that gold adatoms produced by this process form stable thiol-adatom complexes, usually termed "staples" (RS-Auad-SR or RS-Auad-SR-Auad-SR), which are the basic units of the self-assembled monolayers. Here we report on a different scenario for 6-mercaptopurine (6MP), a heterocyclic aromatic thiol, namely its adsorption on the Au(001)-(5 × 20) reconstructed surface. Our results show that 6MP lifts the reconstruction upon adsorption, thus ejecting a large excess of gold adatoms. Surprisingly, 6MP molecules prefer to arrange in highly ordered adatom-free domains in the bridging configuration, while the ejected adatoms form gold islands. Our investigation reveals that the formation of thiol-gold adatom complexes is not always a thermodynamically favored process but rather depends on the nature of the thiol molecule.