Hydride precipitation and stresses in zircaloy-4 observed by synchrotron X-ray diffraction

The grain stresses within hydrides precipitated in rolled zircaloy-4 plates were determined by synchrotron X-ray diffraction experiments using an 80 keV photon beam and a high-speed area detector placed in transmission geometry. Results showed large compressive stresses (360 ± 20 MPa) in the hydride...

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Detalles Bibliográficos
Autores: Santisteban, Javier Roberto, Vicente Alvarez, Miguel Angel, Vizcaino, Pablo, Banchik, A. D., Almer, J. D.
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2010
País:Argentina
Institución:Consejo Nacional de Investigaciones Científicas y Técnicas
Repositorio:CONICET Digital (CONICET)
Idioma:inglés
OAI Identifier:oai:ri.conicet.gov.ar:11336/196605
Acceso en línea:http://hdl.handle.net/11336/196605
Access Level:acceso abierto
Palabra clave:HYDRIDES
INTERNAL STRESSES
PRECIPITATION
TEXTURE
ZIRCONIUM
https://purl.org/becyt/ford/2.5
https://purl.org/becyt/ford/2
Descripción
Sumario:The grain stresses within hydrides precipitated in rolled zircaloy-4 plates were determined by synchrotron X-ray diffraction experiments using an 80 keV photon beam and a high-speed area detector placed in transmission geometry. Results showed large compressive stresses (360 ± 20 MPa) in the hydrides along the plate rolling direction. The origin of these stresses was investigated by performing hydride dissolution/precipitation in situ for thermal cycles between room temperature and 400 C. A large stress hysteresis was observed, with a steady decrease on heating and an abrupt change on cooling. The observed stresses are explained by the constraint imposed by grain boundaries on the growth of hydride platelets on the rolling–transverse plane of the rolled plates.