Processing and characterization of thermoplastic starch/polycaprolactone/compatibilizer ternary blends for packaging applications

Thermoplastic starch (TPS)/polycaprolactone(PCL) blends were obtained by melt mixing. First, thebest formulation of thermoplastic starch (starch, plasticizerand additives) was studied. The obtained filmswere characterized by means of differential scanningcalorimetry, DSC (melting temperature and cry...

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Detalles Bibliográficos
Autores: Guaras, Maria Paula, Alvarez, Vera Alejandra, Ludueña, Leandro Nicolas
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2015
País:Argentina
Institución:Consejo Nacional de Investigaciones Científicas y Técnicas
Repositorio:CONICET Digital (CONICET)
Idioma:inglés
OAI Identifier:oai:ri.conicet.gov.ar:11336/5858
Acceso en línea:http://hdl.handle.net/11336/5858
Access Level:acceso abierto
Palabra clave:Thermoplastic-Starch
Polycaprolactone
Grafting
Mechanical-Properties
Biodegradability
https://purl.org/becyt/ford/2.5
https://purl.org/becyt/ford/2
https://purl.org/becyt/ford/2.4
https://purl.org/becyt/ford/1.4
https://purl.org/becyt/ford/1
Descripción
Sumario:Thermoplastic starch (TPS)/polycaprolactone(PCL) blends were obtained by melt mixing. First, thebest formulation of thermoplastic starch (starch, plasticizerand additives) was studied. The obtained filmswere characterized by means of differential scanningcalorimetry, DSC (melting temperature and crystallinitydegree); thermogravimetric analysis, TGA (real compositionof the blend and thermal stability); tensile tests(mechanical properties); infrared spectroscopy, FTIR(interactions between components); scanning electronmicroscopy, SEM (morphology); and water absorptiontests. The effect of PCL/TPS ratio on the previouslymentioned characteristics and properties were studied.In addition, the effect of using PCL modified withmaleic anhydride as compatibilizer was also analyzed.An optimal compatibilizer content was found improvingthe mechanical properties and slowing down thedegradation rate in soil of the blends. On the otherhand, a slight increase in the water absorption of theblends was found in comparison with the noncompatibilizedones.