Estudio por microscopía electrónica de transmisión de saponita activada.

This work studies the modifications undergone by the Creen Clays Saponite in the Tagus Basin subjected to activation treatments, and stresses the influence of the development of the electronic microscopy technique for studying these materials. Acid treatment with HU and pillaring treatment with Al13...

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Detalhes bibliográficos
Autores: Suárez Barrios, Mercedes, García Romero, Emilia, Santiago Buey, Cristina de, Martín Pozas, José M.
Formato: artículo
Fecha de publicación:1999
País:España
Recursos:Universidad Complutense de Madrid (UCM)
Repositorio:Docta Complutense
Idioma:español
OAI Identifier:oai:docta.ucm.es:20.500.14352/57104
Acesso em linha:https://hdl.handle.net/20.500.14352/57104
Access Level:acceso abierto
Palavra-chave:549.6
Saponite
Acid activation
Pillaring
Transmission electron micróscopy
Cristalografía (Geología)
Descrição
Resumo:This work studies the modifications undergone by the Creen Clays Saponite in the Tagus Basin subjected to activation treatments, and stresses the influence of the development of the electronic microscopy technique for studying these materials. Acid treatment with HU and pillaring treatment with Al13 were performed. Characterization of the samples was carried out by DRX, chemical analysis of majar elements and Transmission Electronic Microscopy. Acid treament causes the delaminarion and fragmentation of the particles, partially dissolving the octahedral layer and generating amorphous silica, coming from the tetrahedral layer. Pillaring treatment gives rise to a stable salid with interlayer spadng at 18A. The high number of crystalline defects present in the saponite conditions the formation of a low number of pillars per cell.